HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Piperidine, acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | 1-Methylpyrrolidine | HCID 8454 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Piperidine, acetate | HCID 9793820 | — |
Reaction Steps
A stock solution of 1 molar piperidine acetate was prepared by mixing one equivalent of glacial acetic acid in an appropriate volume of water and slowly adding one equivalent 1-methylpyrrolidine. The pH of the stock solution is 7. The stock solution was diluted in an appropriate volume of water or acetonitrile to working concentration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07052846B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-40d4c7957bd84867b8718f5c7abb5995 |
| Source note | uspto-grants-2006_05 |