HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22135134, compound → tert-Butyl 4-((methylamino)methyl)piperidine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22135134 | HCID 22135134 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | tert-Butyl 4-((methylamino)methyl)piperidine-1-carboxylate | HCID 21934652 | 106.1% |
Reaction Steps
Using Deprotection Method A, 4-[(N-methyl)benzyloxycarbonylaminomethyl]-1-Boc-piperidine (0.30 g, 0.83 mmol) in EtOAc (5 mL) and EtOH (14 mL) afforded 201 mg (88%) of the title compound which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07053078B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-0ad16b66f4f1454e885de2787ce8e8e0 |
| Source note | uspto-grants-2006_05 |