HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22257623, compound → HCID 22257597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22257623 | HCID 22257623 | — |
| Catalyst | Rhodium | HCID 23948 | — |
| Product | HCID 22257597 | HCID 22257597 | 99% |
Reaction Steps
A solution of 4-(Boc-aminomethyl)pyridine (20 g, 96 mmol) was treated with 5 g of 5% rhodium on carbon and was stirred under 4.1 bar (60 psig) of H2 overnight. Filtration through diatomaceous earth and evaporation of the solvent afforded 20 g (99%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07053078B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-fc59d725b0fc471c94e34676bde10c84 |
| Source note | uspto-grants-2006_05 |