HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Benzyloxybenzyl)benzyl alcohol → 4-(2-Benzyloxybenzyl)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Benzyloxybenzyl)benzyl alcohol | HCID 68872241 | — |
| Catalyst | Manganese oxide | HCID 160959 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-(2-Benzyloxybenzyl)benzaldehyde | HCID 21909304 | 97.6% |
Reaction Steps
To a solution of 4-(2-benzyloxybenzyl)benzyl alcohol (1.0 g) in dichloromethane (50 mL) was added manganese (II) oxide (10 g), and the mixture was stirred at room temperature for 3 hours. An insoluble material was removed by filtration, and the solvent of the filtrate was removed under reduced pressure to give 4-(2-benzyloxybenzyl)benzaldehyde (0.97 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07053060B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-c0f03a660979494594f5cad9c7940123 |
| Source note | uspto-grants-2006_05 |