HuagongsheHuagongshe Chemistry Print Report · For research reference only
Malononitrile → HCID 69620621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Malononitrile | HCID 8010 | — |
| Reactant | 7-Hydroxyindole | HCID 2737651 | — |
| Reactant | 5-Formylpyridine-3-carbonitrile | HCID 12919806 | — |
| Product | HCID 69620621 | HCID 69620621 | 59% |
Reaction Steps
The title compound was prepared from 5-formyl-nicotinonitrile, malononitrile and 7-hydroxyindole by a procedure similar to Example 57 in 59% yield. 1H-NMR (Acetone-d6): 10.54 (brs, 1H), 8.84 (m, J=2.20, 1.90 Hz, 2H), 8.12 (t, J=2.20, 1.90 Hz, 1H), 7.39 (m, J=3.03 Hz, 1H), 7.32 (dd, J=8.00 Hz, 1H), 6.68 (dd, J=8.20 Hz, 1H), 6.51 (m, J=3.03 Hz, 1H), 6.22 (s, 2H), 5.13 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07053117B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-d1a3abf823da4117bc0f19610c1cbe25 |
| Source note | uspto-grants-2006_05 |