Cyclohexene → HCID 23579094, compound

Participants

Reaction Steps

In a stream of nitrogen, 20% palladium hydroxide-carbon (53 mg) and cyclohexene (0.52 ml, 5.1 mmols) were added to an anhydrous ethanol (2 ml) solution of the compound (25) (54 mg, 0.10 mmol), and the mixture was heated under reflux for 2 hours. After filtration, the solvent was distilled off under reduced pressure. The resulting crude product was purified by silica gel column chromatography (chloroform:methanol=80:3) to obtain a white powder (26) (30 mg, 85%).

Provenance & Evidence