HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzylic alcohol → 1,4-Difluoro-2-(3-fluoro-benzyloxy)-5-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzylic alcohol | HCID 68008 | — |
| Reactant | 1,2,4-Trifluoro-5-nitrobenzene | HCID 75012 | — |
| Product | 1,4-Difluoro-2-(3-fluoro-benzyloxy)-5-nitrobenzene | HCID 21920037 | 55% |
Reaction Steps
Prepared in analogy to example 1a) from 2,4,5-trifluoronitrobenzene and 3-fluoro-benzyl alcohol. Colorless solid. Yield=55%. MS: m/e=283.1 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07053245B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-15c68947166e4a5d8e94bd2198d11dc7 |
| Source note | uspto-grants-2006_05 |