4-Nitrobenzenethiol → HCID 22137895, compound

HRID 1827396Notes

Reaction equation

HRID 1827396 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([SH:10])=[CH:6][CH:5]=1)([O-:3])=[O:2].[F:11][C:12]1[CH:13]=[C:14]([CH:17]=[CH:18][CH:19]=1)[CH2:15]Br>>[F:11][C:12]1[CH:19]=[CH:18][CH:17]=[C:14]([CH2:15][S:10][C:7]2[CH:8]=[CH:9][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=2)[CH:13]=1

Participants

3

Reactant 2

HCID 158094-NitrobenzenethiolHCID 680073-Fluorobenzyl bromide

Product 1

HCID 22137895HCID 22137895, compoundYield 54%

Procedure

Prepared in analogy to example 8 from 4-nitrothiophenol and 3-fluoro-benzylbromide. Yellowish solid. Yield=54%.

Sources & evidence

ORD record
ord-de43e29e27d9436296af15d54610f36f
Source dataset
uspto-grants-2006_05
Patent number
US07053245B2

Reaction notes

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