4-Nitrophenol → HCID 22137896, compound

HRID 1827399Notes

Reaction equation

HRID 1827399 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([OH:10])=[CH:6][CH:5]=1)([O-:3])=[O:2].[F:11][C:12]1[CH:19]=[C:18]([F:20])[CH:17]=[CH:16][C:13]=1[CH2:14]Br>>[F:11][C:12]1[CH:19]=[C:18]([F:20])[CH:17]=[CH:16][C:13]=1[CH2:14][O:10][C:7]1[CH:8]=[CH:9][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 9804-NitrophenolHCID 902971-(Bromomethyl)-2,4-difluorobenzene

Product 1

HCID 22137896HCID 22137896, compoundYield 86%

Procedure

Prepared in analogy to example 8 from 4-nitrophenol and 2,4-difluoro-benzylbromide. Colorless solid. Yield=86%. MS: m/e=265.1 (M+).

Sources & evidence

ORD record
ord-229967f4945c4782a677bd587673f236
Source dataset
uspto-grants-2006_05
Patent number
US07053245B2

Reaction notes

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