HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzaldehyde → 4-[2-(3-Fluoro-phenyl)-vinyl]-1-nitro-benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzaldehyde | HCID 68009 | — |
| Reactant | Diethyl 4-nitrobenzylphosphonate | HCID 256065 | — |
| Product | 4-[2-(3-Fluoro-phenyl)-vinyl]-1-nitro-benzene | HCID 68614578 | 82% |
Reaction Steps
Prepared in analogy to example 56b) from (4-nitro-benzyl)-phosphonic acid diethyl ester and 3-fluoro-benzaldehyde. Yellow solid. Yield=82%. MS: m/e=243.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07053245B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-e9811e12382c4ecaa6b90f8fcb09f657 |
| Source note | uspto-grants-2006_05 |