HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzaldehyde → 4-[2-(4-Methoxyphenyl)ethenyl]benzenamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Reactant | Diethyl 4-nitrobenzylphosphonate | HCID 256065 | — |
| Product | 4-[2-(4-Methoxyphenyl)ethenyl]benzenamine | HCID 154910 | 69% |
Reaction Steps
Prepared in analogy to example 56b) from (4-nitro-benzyl)-phosphonic acid diethyl ester and 4-methoxy-benzaldehyde. Yellow solid. Yield=69%. MS: m/e=225.9 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07053245B2 |
| Source dataset | uspto-grants-2006_05 |
| ORD ID | ord-5c918f5b122b47169525b85d680a664d |
| Source note | uspto-grants-2006_05 |