HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Methylamino)ethanol → C7F15C(O)N(CH3)C2H4OH
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Methylamino)ethanol | HCID 8016 | — |
| Reactant | Methyl perfluorooctanoate | HCID 67824 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | C7F15C(O)N(CH3)C2H4OH | HCID 102189403 | 76.4% |
Reaction Steps
C7F15C(O)N(CH3)C2H4OH was prepared by combining n-C7F15CO2CH3 (85 grams) and CH3NHCH2CH2OH (16.5 grams) in THF (50 grams) at 50° C. Progress of the reaction was monitered by GC and FTIR spectra. The isolated yield was 76.4% of C7F15C(O)N(CH3)C2H4OH. (b.p.: 110–125° C./1.5–3 mmHg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07056846B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-1e74967e85b7416aadd933730eb5dc30 |
| Source note | uspto-grants-2006_06 |