HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22065264, compound → HCID 22065266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22065264 | HCID 22065264 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22065266 | HCID 22065266 | — |
Reaction Steps
The title compound was obtained by catalytic hydrogenation of 1-(2,4-dihydroxyphenyl)-2-(3′,4′-dihydroxyphenyl)-1-oxo-2-propene obtained as in Example 3 or Example 4. To a solution of 1-(2,4-dihydroxyphenyl)-2-(3′,4′-dihydroxyphenyl)-1-oxo-2-propene in methanol was added palladium on carbon, and hydrogen gas was bubbled vigorously through the solution for ten minutes. Removal of the catalyst and evaporation of the solvent afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07056952B1 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-1ae7756348d04eba81a2f38945350a32 |
| Source note | uspto-grants-2006_06 |