Phthalimide potassium salt → HCID 69641990, compound

HRID 1828086Notes

Reaction equation

HRID 1828086 reaction equation
[K].[C:2]1(=[O:12])[NH:6][C:5](=[O:7])[C:4]2=[CH:8][CH:9]=[CH:10][CH:11]=[C:3]12.Cl.Cl.[CH2:15]([O:17][C:18](=[O:24])[CH:19](Cl)[O:20][CH2:21][CH3:22])[CH3:16]>>[CH2:15]([O:17][C:18](=[O:24])[CH:19]([N:6]1[C:2](=[O:12])[C:3]2[C:4](=[CH:8][CH:9]=[CH:10][CH:11]=2)[C:5]1=[O:7])[O:20][CH2:21][CH3:22])[CH3:16]

Participants

3

Reactant 2

HCID 24194345Phthalimide potassium saltHCID 87929205HCID 87929205, compound

Product 1

HCID 69641990HCID 69641990, compound

Procedure

According to general procedure A, phthalimide potassium salt was reacted with 2-chloro-2-ethoxyacetic acid ethyl ester dihydrochloride (CAS 172348-75-3) to give (RS)-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethoxy-acetic acid ethyl ester. Light yellow semisolid. MS 278.0 ([M+H]+)

Sources & evidence

ORD record
ord-496351d88ce640639145993be262531e
Source dataset
uspto-grants-2006_06
Patent number
US07056932B2

Reaction notes

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