Potassium bisulfate → Cyclohexene, 4-propyl-

HRID 1828329Notes

Reaction equation

HRID 1828329 reaction equation
[CH2:1]([CH:4]1[CH2:9][CH2:8][CH:7](O)[CH2:6][CH2:5]1)[CH2:2][CH3:3].OS([O-])(=O)=O.[K+].C(OC(=O)C)C.OS([O-])(=O)=O.[K+]>>[CH2:1]([CH:4]1[CH2:9][CH2:8][CH:7]=[CH:6][CH2:5]1)[CH2:2][CH3:3]

Participants

4

Reactant 3

HCID 516920Potassium bisulfateHCID 27750944-PropylcyclohexanolHCID 86585043ethylacetate KHSO4

Product 1

HCID 518777Cyclohexene, 4-propyl-

Conditions

Temperature
70 °C

Procedure

19 g 4-propyl-1-cyclohexanol are mixed with 16 g KHSO4 and stirred for one week at 70° C. After the addition of ethylacetate KHSO4 is filtered off. Ethylacetate is evaporated and the product obtained by fractional distillation.

Workup

  1. filtrationis filtered off
  2. customEthylacetate is evaporated
  3. customthe product obtained by fractional distillation

Sources & evidence

ORD record
ord-fe0d0980757c4a7d9a8a09791b7e7a4a
Source dataset
uspto-grants-2006_06
Patent number
US07057059B2

Reaction notes

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