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HRID1828330

反应详情

EQUATION

反应方程式

HRID 1828330 的结构方程式

REACTANTS

反应物

3
结构：CC(C)(C)C1CCC(O)CC1
HCID7391

4-tert-Butylcyclohexanol

C10H20O

结构：O=S(=O)([O-])O.[K+]
HCID516920

Potassium bisulfate

HKO4S

结构：CCOC(C)=O.O=S(=O)([O-])O.[K+]
HCID86585043

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)C1CC=CCC1
HCID16688

cyclohexene, 4-(1,1-dimethylethyl)-

C10H18

CONDITIONS

反应条件

温度
95 °C

PROCEDURE

实验过程

20 g 4-t-butyl-1-cyclohexanol are mixed with 17 g KHSO4 and stirred for one week at 95° C. After the addition of ethylacetate KHSO4 is filtered off. Ethylacetate is evaporated and the product obtained by fractional distillation.

WORKUP

后处理

  1. filtrationis filtered off
  2. customEthylacetate is evaporated
  3. customthe product obtained by fractional distillation