HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Iodosuccinimide → HCID 12010602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Iodosuccinimide | HCID 120273 | — |
| Reactant | HCID 22066258 | HCID 22066258 | — |
| Product | HCID 12010602 | HCID 12010602 | 43% |
Reaction Steps
N-(1,1-Dimethyl-2-methylthioethyl)-2-nitrobenzamide was treated in the same manner as in Example 19, except that N-iodosuccinimide was used as the iodinating agent, to obtain N-(1,1-dimethyl-2-methylthioethyl)-2-iodo-6-nitrobenzamide (yield 43%, melting point 114–115° C.). Regioselectivity of iodination into the 2-position was 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07057067B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-3652c76750684f40a2fe660ff5e46c63 |
| Source note | uspto-grants-2006_06 |