HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 73863377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | N-Iodosuccinimide | HCID 120273 | — |
| Reactant | HCID 73863378 | HCID 73863378 | — |
| Product | HCID 73863377 | HCID 73863377 | 53% |
Reaction Steps
2-(2-(N-methoxyimino)ethylaminocarbonyl)-2′-methyl-4′-pentafluoroethylbenzanilide was treated in the same manner as in Example 36, except that the N-bromosuccinimide was replaced with N-iodosuccinimide, to obtain 3-iodo-2-(2-(N-methoxyimino)ethylaminocarbonyl)-2′-methyl-4′-pentafluoroethylbenzanilide (yield 53%, melting point 110° C.). Regioselectivity of iodination into the 3-position was 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07057067B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-f503fad969ed4b28afdfed295828c4a3 |
| Source note | uspto-grants-2006_06 |