Cyclohexylamine → N-(Cyclohexyl)-4,5-di-(4-chlorophenyl)-1-methylimidazole-2-carboxamide

Participants

Role	Name	HCID	Charge
Reactant	Cyclohexylamine	HCID 7965	—
Reactant	HCID 22066070	HCID 22066070	—
Product	N-(Cyclohexyl)-4,5-di-(4-chlorophenyl)-1-methylimidazole-2-carboxamide	HCID 10202808	—

Reaction Steps

Using essentially the same procedure as Example 20, Step B, but using cyclohexylamine (0.020 mL, 0.12 mmol), 4,5-di-(4-chlorophenyl)-1-methylimidazole-2-carboxylic acid (20 mg, 0.060 mmol) from Example 20, Step A was converted to the title compound. HPLC/MS: 428 (M+1), 430 (M+3); Rt=4.53 min.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07057051B2
Source dataset	uspto-grants-2006_06
ORD ID	ord-38b53ba3aa994d3daabdf59351dbf6ed
Source note	uspto-grants-2006_06