HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexyl isocyanate → HCID 10226761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexyl isocyanate | HCID 75659 | — |
| Reactant | 4-(4-Chlorophenyl)-5-(2,4-dichlorophenyl)-1-methylimidazole | HCID 22066083 | — |
| Product | HCID 10226761 | HCID 10226761 | — |
Reaction Steps
Using essentially the same procedure as Example 33, but using n-hexyl isocyanate (0.040 mL, 0.30 mmol), 4-(4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-methylimidazole (50 mg, 0.15 mmol) from Example 32, Step C was converted to the title compound after purification twice by Prep TLC (25% ethyl acetate in hexanes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07057051B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-b77ffdec14bc4361b8a15c5b218fb940 |
| Source note | uspto-grants-2006_06 |