Cyclohexylamine → HCID 10227474, compound

Participants

Reaction Steps

Using essentially the same procedure as Example 42, Step C, but using neat cyclohexylamine (2 mL), ethyl 4-(4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-ethylimidazole-2-carboxylate (30 mg, 0.073 mmol) from Example 42, Step B was converted to the title compound after purification by Prep TLC (25% ethyl acetate in hexanes). HPLC/MS: 476 (M+1), 478 (M+3); Rt=5.04 min.

Provenance & Evidence