HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Quinolinecarboxylic acid → HCID 22057947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Quinolinecarboxylic acid | HCID 82571 | — |
| Reactant | N-(3-Amino-4-chlorophenyl)benzamide | HCID 16774920 | — |
| Product | HCID 22057947 | HCID 22057947 | 47% |
Reaction Steps
Using an analogous procedure to that described in Example 7, quinoline-6-carboxylic acid was reacted with N-(3-amino-4-chlorophenyl)benzamide to give the title compound in 47% yield; NMR Spectrum: (DMSOd6) 7.57 (m, 6H), 7.75 (m, 1H), 7.95 (d, 2H), 8.15 (d, 1H), 8.17 (d, 1H), 8.55 (d, 1H), 8.78 (s, 1H), 9.01 (m, 1H), 10.33 (s, 1H), 10.44 (s, 1H); Mass Spectrum: M−H− 400.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07060700B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-b1d68e93925f462da052b3bb03f7f31e |
| Source note | uspto-grants-2006_06 |