HuagongsheHuagongshe Chemistry Print Report · For research reference only
Quinoxaline-6-carboxylic acid → N-[5-(3-cyclohexylpropionamido)-2-methylphenyl]quinoxaline-6-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Quinoxaline-6-carboxylic acid | HCID 674813 | — |
| Reactant | N-(3-amino-4-methylphenyl)-3-cyclohexylpropionamide | HCID 10777768 | — |
| Product | N-[5-(3-cyclohexylpropionamido)-2-methylphenyl]quinoxaline-6-carboxamide | HCID 22057992 | — |
Reaction Steps
Using an analogous procedure to that described in Example 5, quinoxaline-6-carboxylic acid was reacted with N-(3-amino-4-methylphenyl)-3-cyclohexylpropionamide to give the title compound; NMR Spectrum: (DMSOd6) 0.76-0.97 (m, 2H), 1.04-1.24 (m, 3H), 1.40-1.78 (m. 8H), 2.2 (s, 3H), 2.28 (t, 2H), 7.17 (d, 1H), 7.39 (d, 1H), 7.69 (s, 1H), 8.22 (d, 1H), 8.44 (d, 1H), 8.74 (s, 1H), 9.05 (m, 2H), 9.84 (s, 1H), 10.25 (s, 1H); Mass Spectrum: M+H+ 417.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07060700B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-4007dc8270984e04ac0b58e8f2bc6e5d |
| Source note | uspto-grants-2006_06 |