Aniline → HCID 9927213, compound

Participants

Reaction Steps

A solution of 2A (30.0 mg, 0.11 mmol) and aniline (30 μL, 0.33 mmol) in DMF (0.1 mL) was heated at 100° C. for 2.5 h. After the reaction had cooled, the solvent was removed under reduced pressure, and the residue was subjected to preparative HPLC to give 2 as a yellow solid. LC/MS: ret. timeA=3.576 min., MS (M+H)+=324.

Provenance & Evidence