HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dinitrosalicylic acid → 2-Nitrophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dinitrosalicylic acid | HCID 11873 | — |
| Reactant | Diisopropylcarbodiimide | HCID 12734 | — |
| Reactant | 1-Hydroxybenzotriazole | HCID 75771 | — |
| Product | 2-Nitrophenol | HCID 6947 | — |
Reaction Steps
This material was prepared from 3,5-dinitrosalicylic acid (1d) (1 g, 4.4 mmol), HOBt (1 g, 7.4 mmol), DIC (1,3-diisopropylcarodiimide, 1 mL, 6.4 mmol), and an amino macroporous resin (1 g, 0.4 mmol) using a procedure similar to polystyrene resin (PS-2a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07060752B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-8c38edad6ed444a5abd7852b488747a5 |
| Source note | uspto-grants-2006_06 |