Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | 2-Chlorobenzimidazole | HCID 78572 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2,5-Dichlorobenzimidazole | HCID 335473 | 37.3% |
Reaction Steps
2-Chlorobenzimidazole (1.05 g) was dissolved in DMF (10 mL), and N-chlorosuccinimide (1.01 g) was added thereto. The mixture was stirred at 60° C. for 30 min and the reaction mixture was added to water. The precipitated solid was collected by filtration to give 2,5-dichlorobenzimidazole (0.480 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07060722B2 |
|---|
| Source dataset | uspto-grants-2006_06 |
|---|
| ORD ID | ord-00c9127842f44f6caf206623c7596177 |
|---|
| Source note | uspto-grants-2006_06 |
|---|
