HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 86587920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 3-(2-methyl-1H-imidazol-1-yl)propan-1-amine | HCID 3152105 | — |
| Product | HCID 86587920 | HCID 86587920 | 95.7% |
Reaction Steps
60.0 g of urea was added to 139.2 g of 1-(3′-aminopropyl)-2-methylimidazole and reacted at 160° C. for 10 hours, and after the reaction, a volatile component was removed to obtain 176.1 g of a 1-{3′-(2″-methylimidazolinyl)propyl)urea composition. 117.4 g of dipropylene glycol was added thereto to prepare a solution containing 60% of a 1-(3′-(2″-methylimidazolinyl)propyl}urea composition (IZUM), which was subjected to the following foaming test. The composition of the solution is shown in Table 17.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07064172B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-f0139f14041849c796408afc1621261b |
| Source note | uspto-grants-2006_06 |