反应详情

温度

180 °C

The mixture of 1,1-bis(4-fluorophenyl)-1,2-ethanediamine(153 mg) and 4-cyano-2-ethoxycarbonylpyridine(95 mg) was stirred at 180° C. for 2 hours. The obtained oily compound was purified by silica gel column chromatography (C-300; hexane:ethyl acetate=3:2) to give the objective compound (103 mg).

1. customThe obtained oily compound was purified by silica gel column chromatography (C-300; hexane:ethyl acetate=3:2)