HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Pentanol → Amyl oleate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Pentanol | HCID 6276 | — |
| Reactant | Ethyl Oleate | HCID 5363269 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Amyl oleate | HCID 5354230 | 91% |
Reaction Steps
A mixture containing Catalyst A or B (0.05 g) and ethyl oleate (1.55 g, 5 mmol) and pentanol (10 ml) was refluxed with stirring for 40 h. On cooling ether (30 ml) was added and the catalyst was filtered off. The organic washings were combined and concentrated to give pentyl oleate as an oil (1.6 g, 91% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07064226B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-a81f94ef2f664c7583f8206b6b274013 |
| Source note | uspto-grants-2006_06 |