HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzylic alcohol → 4-Fluorobenzoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzylic alcohol | HCID 68022 | — |
| Reactant | Sodium Bromate | HCID 23668195 | — |
| Solvent | Acetonitrile--water (1/1) | HCID 18373917 | — |
| Product | 4-Fluorobenzoic Acid | HCID 9973 | 89.7% |
Reaction Steps
The separated catalyst was added to a fresh batch of sodium bromate (0.3 g) and 4-fluorobenzyl alcohol (0.256 g, 2 mmol) in acetonitrile:water (1:1, 10 ml). The above procedure was repeated to give 4-fluorobenzoic acid as a white solid (0.25 g, 88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07064226B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-6e1db53bb1d6479284a460a0dd7f4a63 |
| Source note | uspto-grants-2006_06 |