HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl-(2-{[1-(5-nitro-1H-indol-2-yl)-methanoyl]-amino}-ethyl)-carbamic acid dimethyl-ethyl ester → (2-{[1-(5-Nitro-1H-indol-2-yl)-methanoyl]-amino}-ethyl)-propyl-carbamic acid dimethyl-ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl-(2-{[1-(5-nitro-1H-indol-2-yl)-methanoyl]-amino}-ethyl)-carbamic acid dimethyl-ethyl ester | HCID 67550180 | — |
| Reactant | 5-Nitro-1H-indole-2-carboxylic acid (2-propylamino-ethyl)-amide | HCID 85801385 | — |
| Product | (2-{[1-(5-Nitro-1H-indol-2-yl)-methanoyl]-amino}-ethyl)-propyl-carbamic acid dimethyl-ethyl ester | HCID 67550175 | 88% |
Reaction Steps
A similar procedure as described for preparation of 78 from compound 81 (0.12 g, 0.413 mmol) gave brown powder (0.142 g, 88%). ESI MS: 391.17 (M+H+), 413.15 (M+Na+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07064218B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-f6c8b622baa34850a9bccd450f085c5f |
| Source note | uspto-grants-2006_06 |