4-(4-Methylpiperazino)-1,2-benzenediamine → HCID 135820115, compound

HRID 1830016Notes

Reaction equation

HRID 1830016 reaction equation
[N+:1]([C:4]1[CH:5]=[CH:6][C:7]([O:10][C:11]2[CH:12]=[C:13]3[C:17](=[CH:18][CH:19]=2)[NH:16][N:15]=[C:14]3[CH:20]=O)=[N:8][CH:9]=1)([O-:3])=[O:2].[CH3:22][N:23]1[CH2:28][CH2:27][N:26]([C:29]2[CH:30]=[C:31]([NH2:36])[C:32]([NH2:35])=[CH:33][CH:34]=2)[CH2:25][CH2:24]1>>[CH3:22][N:23]1[CH2:24][CH2:25][N:26]([C:29]2[CH:34]=[CH:33][C:32]3[N:35]=[C:20]([C:14]4[C:13]5[C:17](=[CH:18][CH:19]=[C:11]([O:10][C:7]6[CH:6]=[CH:5][C:4]([N+:1]([O-:3])=[O:2])=[CH:9][N:8]=6)[CH:12]=5)[NH:16][N:15]=4)[NH:36][C:31]=3[CH:30]=2)[CH2:27][CH2:28]1

Participants

3

Reactant 2

HCID 27635454-(4-Methylpiperazino)-1,2-benzenediamineHCID 178520038HCID 178520038, compound

Product 1

HCID 135820115HCID 135820115, compound

Procedure

The title compound was synthesized from 5-(5-nitro-pyridin-2-yloxy)-1H-indazole-3-carbaldehyde and 4-(4-methyl-piperazin-1-yl)-benzene-1,2-diamine using the method described above in Example 4. LC/MS (m/z) 471.3 (MH+), Rt 2.94 minutes.

Sources & evidence

ORD record
ord-074b60bc0d814fb29184c3b61e572353
Source dataset
uspto-grants-2006_06
Patent number
US07064215B2

Reaction notes

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