Dimethylamine → HCID 22049729, compound

HRID 1830879Notes

Reaction equation

HRID 1830879 reaction equation
[I:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][C:10]=1[CH3:11])[C:5](Cl)=[O:6].[CH3:12][NH:13][CH3:14]>>[I:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][C:10]=1[CH3:11])[C:5]([N:13]([CH3:14])[CH3:12])=[O:6]

Participants

3

Reactant 2

HCID 674DimethylamineHCID 177521573-Iodo-4-methylbenzoyl chloride

Product 1

HCID 22049729HCID 22049729, compound

Procedure

By the reaction in the same manner as in Example 27-i) using 3-iodo-4-methylbenzoyl chloride (2.00 g) and 50% aqueous dimethylamine solution (20 ml), the title compound (1.72 g) was obtained as a pale-yellow oil.

Workup

  1. customBy the reaction in the same manner as in Example 27-i)

Sources & evidence

ORD record
ord-412ea180e0c34c82b317218a1325e968
Source dataset
uspto-grants-2006_06
Patent number
US07067537B2

Reaction notes

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