Bromine → HCID 22049763, compound

HRID 1830898Notes

Reaction equation

HRID 1830898 reaction equation
[CH3:1][CH:2]([CH3:13])[CH2:3][C:4]([C:6]1[CH:7]=[N:8][CH:9]=[CH:10][C:11]=1[CH3:12])=[O:5].[Br:14]Br>>[Br:14][CH:3]([CH:2]([CH3:13])[CH3:1])[C:4]([C:6]1[CH:7]=[N:8][CH:9]=[CH:10][C:11]=1[CH3:12])=[O:5]

Participants

3

Reactant 2

HCID 24408BromineHCID 220498061-Butanone, 3-methyl-1-(4-methyl-3-pyridinyl)-

Product 1

HCID 22049763HCID 22049763, compoundYield 85.9%

Procedure

By the reaction in the same manner as in Example 53-ii) using 3-methyl-1-(4-methylpyridin-3-yl)butan-1-one (3.10 g) and bromine (2.68 g), the title compound (3.69 g) was obtained as a pale-yellow powder.

Workup

  1. customBy the reaction in the same manner as in Example 53-ii)

Sources & evidence

ORD record
ord-26f0491e2ca84a629e5c2a2654d2c560
Source dataset
uspto-grants-2006_06
Patent number
US07067537B2

Reaction notes

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