HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Sulfamoylthiobenzamide → 4-[5-Methyl-4-(4-methylpyridin-3-yl)-1,3-thiazol-2-yl]benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Sulfamoylthiobenzamide | HCID 3003266 | — |
| Reactant | 2-Bromo-1-(4-methylpyridin-3-yl)propan-1-one | HCID 22049762 | — |
| Product | 4-[5-Methyl-4-(4-methylpyridin-3-yl)-1,3-thiazol-2-yl]benzenesulfonamide | HCID 22049755 | 56.8% |
Reaction Steps
By the reaction in the same manner as in Example 25-iii) using 2-bromo-1-(4-methylpyridin-3-yl)propan-1-one hydrobromate (510 mg) and 4-(aminosulfonyl)benzenecarbothioamide (355 mg), the title compound (322 mg) was obtained as colorless powder crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067537B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-ce545a3b15d4460abeb2f3e5f13ee968 |
| Source note | uspto-grants-2006_06 |