Bromine → 2-Bromo-1-(4-ethylpyridin-3-yl)ethanone

HRID 1830908Notes

Reaction equation

HRID 1830908 reaction equation
[CH2:1]([C:3]1[CH:8]=[CH:7][N:6]=[CH:5][C:4]=1[C:9](=[O:11])[CH3:10])[CH3:2].[Br:12]Br>>[Br:12][CH2:10][C:9]([C:4]1[CH:5]=[N:6][CH:7]=[CH:8][C:3]=1[CH2:1][CH3:2])=[O:11]

Participants

3

Reactant 2

HCID 24408BromineHCID 217660071-(4-Ethylpyridin-3-YL)ethanone

Product 1

HCID 220497942-Bromo-1-(4-ethylpyridin-3-yl)ethanoneYield 85.4%

Procedure

By the reaction in the same manner as in Example 53-ii) using 1-(4-ethylpyridin-3-yl)ethanone (1.68 g) and bromine (1.60 g), the title compound (1.95 g) was obtained as a pale-brown powder.

Workup

  1. customBy the reaction in the same manner as in Example 53-ii)

Sources & evidence

ORD record
ord-5bcaeca7a3254366872f10a61f532b52
Source dataset
uspto-grants-2006_06
Patent number
US07067537B2

Reaction notes

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