HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethyl)pyridine-3-carbothioamide → HCID 22049737, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethyl)pyridine-3-carbothioamide | HCID 2777771 | — |
| Reactant | 2-bromo-1-(3-bromo-4-fluorophenyl)ethanone | HCID 2782783 | — |
| Product | HCID 22049737 | HCID 22049737 | 41% |
Reaction Steps
By the reaction in the same manner as in Example 25-iii) using 2-bromo-1-(3-bromo-4-fluorophenyl)ethanone (3.10 g) and 4-trifluoromethylpyridine-3-thiocarboxamide (1.87 g), the title compound (1.50 g) was obtained as brown needle crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067537B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-f602b7b88b024fa5843c47a68e206547 |
| Source note | uspto-grants-2006_06 |