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HRID1831084

反应详情

EQUATION

反应方程式

HRID 1831084 的结构方程式

REACTANTS

反应物

2
结构：CN(C(=O)Cl)c1ccccc1
HCID77969

Carbamic chloride, methylphenyl-

C8H8ClNO

结构：N#Cc1ncc(C(F)(F)F)cc1Oc1ccc(O)cc1
HCID4313863

未命名化合物

PRODUCTS

生成物

1
结构：CN(C(=O)Oc1ccc(Oc2cc(C(F)(F)F)cnc2C#N)cc1)c1ccccc1
HCID10309896

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(2-cyano-5-trifluoromethyl-pyridin-3-yloxy)-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was purified by preparative HPLC (74%, colourless oil). HPLC-MS m/z=414.1 (M+1), Rt: 4.8 min.

WORKUP

后处理

  1. customThe crude product was purified by preparative HPLC (74%, colourless oil)