Carbamic chloride, N-methyl-N-phenyl- → HCID 1306380, compound

HRID 1831089Notes

Reaction equation

HRID 1831089 reaction equation
[Cl:1][C:2]1[CH:16]=[CH:15][C:5]([C:6]([C:8]2[CH:13]=[CH:12][C:11]([OH:14])=[CH:10][CH:9]=2)=[O:7])=[CH:4][CH:3]=1.[CH3:17][N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](Cl)=[O:20]>>[Cl:1][C:2]1[CH:16]=[CH:15][C:5]([C:6]([C:8]2[CH:13]=[CH:12][C:11]([O:14][C:19](=[O:20])[N:18]([CH3:17])[C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)=[CH:10][CH:9]=2)=[O:7])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 1235044-Hydroxy-4'-chlorobenzophenone

Product 1

HCID 1306380HCID 1306380, compound

Procedure

The title compound was prepared from 4-(4-chlorobenzoyl)-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was recrystallized (ethanol/water) (90%, white crystals). HPLC-MS m/z=366.1 (M+1), Rt: 5.19 min.

Workup

  1. customThe crude product was recrystallized (ethanol/water) (90%, white crystals)

Sources & evidence

ORD record
ord-8b70774fa0df4b2ea28aa3e363a83a78
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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