Carbamic chloride, N-methyl-N-phenyl- → HCID 10149470, compound

HRID 1831091Notes

Reaction equation

HRID 1831091 reaction equation
[N:1]1([C:6]2[CH:11]=[CH:10][C:9]([OH:12])=[CH:8][CH:7]=2)[CH:5]=[CH:4][CH:3]=[CH:2]1.[CH3:13][N:14]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[C:15](Cl)=[O:16]>>[N:1]1([C:6]2[CH:11]=[CH:10][C:9]([O:12][C:15](=[O:16])[N:14]([CH3:13])[C:18]3[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=3)=[CH:8][CH:7]=2)[CH:2]=[CH:3][CH:4]=[CH:5]1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 90072p-(1H-Pyrrol-1-yl)phenol

Product 1

HCID 10149470HCID 10149470, compound

Procedure

The title compound was prepared from 4-pyrrol-1-yl-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was recrystallized (ethanol/water) (27%, off-white crystals). HPLC-MS m/z=293.2 (M+1), Rt: 4.51 min.

Workup

  1. customThe crude product was recrystallized (ethanol/water) (27%, off-white crystals)

Sources & evidence

ORD record
ord-066da8b38de44d0dacff68b1724e646a
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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