Monobenzone → HCID 10215274, compound

HRID 1831094Notes

Reaction equation

HRID 1831094 reaction equation
[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:16][N:17]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)[C:18](Cl)=[O:19]>>[CH2:1]([O:8][C:9]1[CH:10]=[CH:11][C:12]([O:15][C:18](=[O:19])[N:17]([CH3:16])[C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)=[CH:13][CH:14]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 7638MonobenzoneHCID 77969Carbamic chloride, N-methyl-N-phenyl-

Product 1

HCID 10215274HCID 10215274, compound

Procedure

The title compound was prepared from 4-benzyloxy-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was recrystallized (ethanol/water) (83%, white crystals). HPLC-MS m/z=334.2 (M+1), Rt: 4.88 min.

Workup

  1. customThe crude product was recrystallized (ethanol/water) (83%, white crystals)

Sources & evidence

ORD record
ord-9948486b4d404e2194a74d36295e3098
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

Loading…