Carbamic chloride, N-methyl-N-phenyl- → HCID 10172913, compound

HRID 1831098Notes

Reaction equation

HRID 1831098 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9](=[O:18])[NH:10][C:11]2[CH:16]=[CH:15][C:14]([OH:17])=[CH:13][CH:12]=2)=[CH:4][CH:3]=1.[CH3:19][N:20]([C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1)[C:21](Cl)=[O:22]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([NH:8][C:9](=[O:18])[NH:10][C:11]2[CH:16]=[CH:15][C:14]([O:17][C:21](=[O:22])[N:20]([CH3:19])[C:24]3[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=3)=[CH:13][CH:12]=2)=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 854443HCID 854443, compound

Product 1

HCID 10172913HCID 10172913, compound

Procedure

The title compound was prepared from 4-[3-(4-chlorophenyl)-ureido]-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (33%, off-white crystals). HPLC-MS m/z=396.1 (M+1), Rt: 4.40 min.

Sources & evidence

ORD record
ord-3e14053b3d7f40eca192d8a9657f2df9
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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