HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 4-(4-nitro-phenoxy)-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Reactant | 4-(4-Nitrophenoxy)phenol | HCID 152450 | — |
| Product | Methyl-phenyl-carbamic Acid 4-(4-nitro-phenoxy)-phenyl Ester | HCID 10215649 | — |
Reaction Steps
The title compound was prepared from 4-(4-nitro-phenoxy)-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (71%, white crystals). HPLC-MS m/z=365.0 (M+1), Rt: 4.83 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-6174b3c5bbff46009a0a5af7620521e4 |
| Source note | uspto-grants-2006_06 |