Carbamic chloride, N-methyl-N-phenyl- → HCID 10172359, compound

HRID 1831100Notes

Reaction equation

HRID 1831100 reaction equation
[CH2:1]([S:8][C:9]1[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[CH3:16][N:17]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)[C:18](Cl)=[O:19]>>[CH2:1]([S:8][C:9]1[CH:14]=[CH:13][C:12]([O:15][C:18](=[O:19])[N:17]([CH3:16])[C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 361428341796-12-7

Product 1

HCID 10172359HCID 10172359, compound

Procedure

The title compound was prepared from 4-heptylsulfanyl-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (74%, colourless oil, HPLC-MS m/z=358.2 (M+1), Rt: 6.21 min.

Sources & evidence

ORD record
ord-5bc081b20b064cc79aaf71675a18a4b8
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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