HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Butoxyphenol → Methyl-phenyl-carbamic acid 4-butoxy-phenyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Butoxyphenol | HCID 31233 | — |
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Product | Methyl-phenyl-carbamic acid 4-butoxy-phenyl ester | HCID 10286290 | — |
Reaction Steps
The title compound was prepared from 4-butoxy-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was recrystallized from ethanol (22%, white crystals). HPLC-MS m/z=300.1 (M+1), Rt: 5.20.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-ea14affbda464fbba7523aa423c5b6d7 |
| Source note | uspto-grants-2006_06 |