HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-methyl-3-(methyl-phenyl-carbamoyl)-3H-imidazol-1-ium iodide → Methyl-phenyl-carbamic Acid 4-(4,4-dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-methyl-3-(methyl-phenyl-carbamoyl)-3H-imidazol-1-ium iodide | HCID 10947884 | — |
| Reactant | 1-(4-Hydroxyphenyl)-4,4-dimethylpiperidine-2,6-dione | HCID 22047742 | — |
| Product | Methyl-phenyl-carbamic Acid 4-(4,4-dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl Ester | HCID 10126229 | — |
Reaction Steps
The title product was prepared from 1-(4-hydroxyphenyl)-4,4-dimethylpiperidine-2,6-dione (233 mg, 1.00 mmol) ) and 1-methyl-3-(methyl-phenyl-carbamoyl)-3H-imidazol-1-ium iodide (343 mg, 1.00 mmol) by applying general procedure 3 (192 mg, 52%, white solid). HPLC-MS m/z=367 (M+1); Rt=3.78 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-72a924dafd034d0c9de9bf63e3077621 |
| Source note | uspto-grants-2006_06 |