HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(4-hydroxyphenyl)cyclohexanecarboxamide → Methyl-phenyl-carbamic Acid 4-(cyclohexanecarbonyl-amino)-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(4-hydroxyphenyl)cyclohexanecarboxamide | HCID 4056004 | — |
| Reactant | 1-methyl-3-(methyl-phenyl-carbamoyl)-3H-imidazol-1-ium iodide | HCID 10947884 | — |
| Product | Methyl-phenyl-carbamic Acid 4-(cyclohexanecarbonyl-amino)-phenyl Ester | HCID 10193633 | 80.3% |
Reaction Steps
The title compound (283 mg, 80% yield, white crystals) was prepared from cyclohexanecarboxylic acid (4-hydroxyphenyl) amide (219 mg, 1.00 mmol) and 1-methyl-3-(methyl-phenyl-carbamoyl)-3H-imidazol-1-ium iodide (343 mg, 1.00 mmol). HPLC-MS m/z=353 (M+1); Rt=4.23 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-add363caa7f0458c8d2654d16d428a7c |
| Source note | uspto-grants-2006_06 |