Ethyl(phenyl)carbamoyl chloride → Ethyl-phenyl-carbamic Acid 4-(4-trifluoromethyl-phenoxy)-phenyl Ester

HRID 1831122ノート

反応式

HRID 1831122 の反応式
[F:1][C:2]([F:18])([F:17])[C:3]1[CH:16]=[CH:15][C:6]([O:7][C:8]2[CH:13]=[CH:12][C:11]([OH:14])=[CH:10][CH:9]=2)=[CH:5][CH:4]=1.[CH2:19]([N:21]([C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1)[C:22](Cl)=[O:23])[CH3:20]>>[F:1][C:2]([F:17])([F:18])[C:3]1[CH:16]=[CH:15][C:6]([O:7][C:8]2[CH:9]=[CH:10][C:11]([O:14][C:22](=[O:23])[N:21]([CH2:19][CH3:20])[C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)=[CH:12][CH:13]=2)=[CH:5][CH:4]=1

参加物

3

反応物 2

HCID 96376Ethyl(phenyl)carbamoyl chlorideHCID 170230p-(4-(Trifluoromethyl)phenoxy)phenol

生成物 1

HCID 10150786Ethyl-phenyl-carbamic Acid 4-(4-trifluoromethyl-phenoxy)-phenyl Ester

実験手順

The title compound was prepared from 4-(4-trifluoromethyl-phenoxy)-phenol and N-ethyl-N-phenylcarbamoyl chloride. The crude product was subjected to flash chromatography (ethyl

出典と根拠

ORDレコード
ord-86f8947e699c4fe5a9e05861ab673ef4
出典データセット
uspto-grants-2006_06
特許番号
US07067517B2

反応ノート

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