HRID1831135

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID155241

4-[[5-(Trifluoromethyl)-2-pyridinyl]oxy]phenol

C12H8F3NO2

结构：C[n+]1ccn(C(=O)N2CCC(Cc3ccccc3)CC2)c1.[I-]

HCID86589190

未命名化合物

PRODUCTS

生成物

结构：O=C(Oc1ccc(Oc2ccc(C(F)(F)F)cn2)cc1)N1CCC(Cc2ccccc2)CC1

HCID23635636

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenol and 1-methyl-3-(4-benzyl-piperidine-1-carbonyl)-3H-imidazol-1-ium iodide. The crude product was purified by flash chromatography using a Quad flash 25 (ethyl acetate/heptane (1:6), (72%, white crystals). HPLC-MS m/z=457.2 (M+1), Rt: 6.0 min.

WORKUP

后处理

customThe crude product was purified by flash chromatography