HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 3-(4-methoxy-phenyl)-pyrazol-1-yl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Reactant | 1-Hydroxy-3-(4-methoxyphenyl)pyrazole | HCID 11805519 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | Methyl-phenyl-carbamic Acid 3-(4-methoxy-phenyl)-pyrazol-1-yl Ester | HCID 10236710 | — |
Reaction Steps
The title compound was prepared from 1-hydroxy-3-(4-methoxyphenyl)pyrazole and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to flash chromatography (Quad flash 25, EtOAc-heptane) (93%, oil). HPLC-MS m/z=346.1 (M+Na), Rt: 4.21 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-1507cb23d76f470bb3dbe04b33335183 |
| Source note | uspto-grants-2006_06 |